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Publication No: IN202311018071 [India] Application No: IN202311018071
Title: A continuous process for purification of bisphenol - A
Publication Date: 20-09-2024 File Date: 15-03-2023
Inventor(s): Sanjay Pandurang Kamble; Sunil Sitaram Bhongale; Kapil Dnyaneshwar Dhotre; Narendra Balwant Bodawar
IPC Classification: C07C37/72, C07C27/00
Abstract:
The present invention relates to purification of bisphenol and/or its analogues and isomers. Specifically, the present invention relates to a continuous process for the  purification of bisphenol-A (BPA) utilizing flash distillation and agitated thin film evaporator (ATFE) /agitated thin film dryer (ATFD) wherein unreacted phenol and  traces of acetone are recovered and reused. Further impurities present in the crude BPA were selectively removed by combination of organic and aqueous solvent to  obtain the highly pure and colorless BPA. Another advantage present invention is the use of minimum quantity water (crude BPA to water ratio wt 1: 1) in the  downstream processing of crude BPA and the wastewater generated was further treated using cavitation/adsorption/ advanced oxidation processes (AOPs) and hybrid  AOPs techniques. The purified water further can be used in the process or as plant utilities like cooling water, boiler water, plant cleaning water etc.
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Industrial Applications Chemistry, Chemical Processes Polymers [Chemistry, Chemical Processes] Water treatment [Environmental (Clean Tech)]