New Invention Profile
| Publication No: | IN202311022579 [India] | Application No: | IN202311022579 |
| Title: | A process for the isomerization of ENDO-THDCPD into EXO- THDCPD (JP-10) using isolated AlCl3 monomer | ||
| Publication Date: | 11-10-2024 | File Date: | 28-03-2023 |
| Inventor(s): | ANIL KUMAR SINHA; ROHIT KUMAR; SALEEM AKTHAR FAROOQUI; RAKESH KUMAR; AZEEM KHAN | ||
| IPC Classification: | A61P 27/16, H04L 9/40, C07C 5/27, H04L 69/329, H02J 3/38 | ||
| Abstract: | The present inventors have found that under conditions of monomeric AlCl3 in the reaction medium, it is possible that with a minimum amount of AlCl3 in the isomerization reaction of Endo-THDCPD to Exo-THDCPD, obtained product purity for Exo-THDCPD (99.2%) was better than the purity required for JP-10 (98.5%). Specifically, the present inventors have confirmed the optimum reaction conditions, temperature (23.5 degree C), 1 wt% of AlCl3, 500 RPM stirring speed and 1 hour reaction time for the above-said reaction Endo-THDCPD to Exo-THDCPD. Scale-up of the process is also confirmed by the experiments. The product purity was similar after the scale-up. |
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