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Publication No: IN202211039599 [India] Application No: 202211039599
Title: A process for the synthesis of fluorescent silica nanoparticles from fly ash
Publication Date: 12-01-2024 File Date: 08-07-2022
Inventor(s): Vikram Singh; Hridesh Agarwalla; Reginald Ebhin Masto; Manish Kumar
IPC Classification: B82Y30/00, C09K11/06, H01L51/00, C08G83/00, G01N21/64
Abstract: The present invention  relates to one-step hydrothermal synthesis of water-soluble, crystalline, blue-emitting, fluorescent amine-functionalized silica  nanoparticles (SiNPs) from coal fly ash. Tertiary amine (trimethylamine) was used for the preparation of amine-functionalized  fluorescent SiNPs particularly to enhance the fluorescence property. The FESEM and TEM study showed that the diameter of SiNPs  is in the range of 5-15 nm with spherical morphology. The XPS and FTIR study revealed the presence of amine groups at the surface  of SiNPs. The SiNPs exhibited blue fluorescence with an emission maximum at 454 nm at an excitation wavelength of 370 nm in an  aqueous medium. They displayed excitation-dependent emission property. The SiNPs were functionalized with amine group that  enable their use in biomedical applications such as imaging and targeted drug delivery. They are also suitable for other applications  such as sensing, light-emitting device and light-harvesting.
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Industrial Applications Chemistry, Chemical Processes Polymers [Chemistry, Chemical Processes] Materials Processes [Materials] Nanomaterials [Materials]